Solid-phase extraction and concentration of trace chlorophenols with extractant- impregnated membrane disks
نویسندگان
چکیده
منابع مشابه
Ethanol/Water extraction combined with solid-phase extraction and solid-phase microextraction concentration for the determination of chlorophenols in cork stoppers.
The appearance of 2,4,6-trichloroanisole (TCA) in cork stoppers is of great concern because it can cause off-flavors in bottled wine. To prevent this sensorial defect, there should not be any traces of 2,4,6-trichlorophenol (TCP), 2,3,4,6-tetrachlorophenol (TeCP), or pentachlorophenol (PCP) in the finished corks, because they are the direct precursors of TCA. In the course of this study two met...
متن کاملReview of preconcentration and solid phase extraction for the determination of trace Lead
Spectrometric techniques for the analysis of trace lead have developed rapidly due to the increasing need for accurate measurements at extremely low levels of this element in diverse matrices. This review covers separation and preconcentration procedures, and considers the features of the application with several spectrometric techniques. The use of an appropriate sample handling technique is a...
متن کاملReview of preconcentration and solid phase extraction for the determination of trace Lead
Spectrometric techniques for the analysis of trace lead have developed rapidly due to the increasing need for accurate measurements at extremely low levels of this element in diverse matrices. This review covers separation and preconcentration procedures, and considers the features of the application with several spectrometric techniques. The use of an appropriate sample handling technique is a...
متن کاملSolid Phase Extraction of Ultra Trace Amounts of Ni2+ by Dimethylglyoxime (DMG) Immobilized on Column
A column of alumina modified with sodium dodecyl sulfate (SDS) and dimethylglyoxime (DMG) was prepared for the preconcentration of trace nickel from water samples for flame atomic absorption spectrometry (FAAS) determinations. Under optimized conditions (pH=7.0; flow rate: 20 mlmin-1) nickel was retained on the column. The nickel collected on the column was eluted with 5 mL of 1 M nitric ac...
متن کاملsolid phase extraction of trace copper in aqueous samples using c18 membrane disks modified by benzildithiosemicarbazone prior to flame atomic absorption spectrometric (faas) determination
a highly convenient, selective and sensitive procedure for pre-concentration, separation and determination of sub-ppm levels of cu 2+ in aqueous samples based on modification of octadecyl silica bonded phase membrane (osbpm) disks is described using benzildithiosemicarbazone (bdsc) as a powerful modifier. it was revealed that each loaded osbpm disk with 6.0 mg of bdsc serves as excellent bead ...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: BUNSEKI KAGAKU
سال: 2003
ISSN: 0525-1931
DOI: 10.2116/bunsekikagaku.52.825